HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-(3,5-Dimethylphenyl)piperazine → HCID 52948333, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-(3,5-Dimethylphenyl)piperazine | HCID 2758626 | — |
| Reactant | Ethyl N-(2,6-dimethoxyquinoxalin-3-yl)carbamate | HCID 66918080 | — |
| Product | HCID 52948333 | HCID 52948333 | 65% |
Reaction Steps
Ethyl N-(2,6-dimethoxyquinoxalin-3-yl)carbamate and 1-(3,5-dimethylphenyl)piperazine were reacted by the same way with the example 64 to obtain the titled compound (yield, 65%). 1H NMR (300 MHz, CDCl3): δ 2.28 (s, 6H), 3.26 (s, 4H), 3.76-3.87 (m, 6H), 4.11 (s, 4H), 6.59 (s, 2H), 6.90 (m, 1H), 7.14 (d, J=8.7 Hz, 1H), 7.32 (s, 1H), 7.51 (d, J=7.5 Hz, 1H), 7.64 (d, J=8.7 Hz, 1H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08314100B2 |
| Source dataset | uspto-grants-2012_11 |
| ORD ID | ord-a248813f70f84590934c9b53df2d5d4f |
| Source note | uspto-grants-2012_11 |