HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-(2-Cyanophenyl)piperazine → HCID 66918223, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-(2-Cyanophenyl)piperazine | HCID 2735875 | — |
| Reactant | Ethyl N-(2,6-dimethoxyquinoxalin-3-yl)carbamate | HCID 66918080 | — |
| Product | HCID 66918223 | HCID 66918223 | 94% |
Reaction Steps
Ethyl N-(2,6-dimethoxyquinoxalin-3-yl)carbamate and 1-(2-cyanophenyl)piperazine were reacted by the same way with the example 64 to obtain the titled compound (yield, 94%). 1H NMR (200 MHz, CDCl3): δ 3.30 (s, 4H), 3.88-3.90 (m, 6H), 4.07-4.20 (m, 4H), 6.94-7.07 (m, 3H), 7.27-7.34 (m, 2H), 7.53-7.63 (m, 3H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08314100B2 |
| Source dataset | uspto-grants-2012_11 |
| ORD ID | ord-0d983070e0b94fc28bdb456db3b8d34d |
| Source note | uspto-grants-2012_11 |