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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1878192Generated: November 1, 2026

2-Mepp → HCID 69243672, compound

https://huagongshe.com/reaction/1878192

Reaction equation

Participants

RoleNameHCIDCharge
Reactant2-MeppHCID 91965—
Reactantethyl N-(6-fluoro-3-methoxyquinoxalin-2-yl)carbamateHCID 69243333—
ProductHCID 69243672HCID 6924367277%

Reaction Steps

Ethyl N-(6-fluoro-3-methoxyquinoxalin-2-yl)carbamate and 1-(2-methylphenyl)piperazine were reacted by the same way with the example 85 to obtain the titled compound (yield, 77%). 1H NMR (200 MHz, CDCl3): δ 2.95 (s, 3H), 2.99-3.02 (m, 4H), 3.74-3.77 (m, 4H), 4.15 (s, 3H), 7.01-7.05 (m, 2H), 7.17-7.42 (m, 5H), 7.81-7.84 (m, 1H).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08314100B2
Source datasetuspto-grants-2012_11
ORD IDord-c024ff12ed7e4169bf9fc664cf63c5c2
Source noteuspto-grants-2012_11