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HRID1878271

反应详情

EQUATION

反应方程式

HRID 1878271 的结构方程式

REACTANTS

反应物

2
结构：O=[N+]([O-])c1ccc(N2CCNCC2)cc1
HCID80447

1-(4-Nitrophenyl)piperazine

C10H13N3O2

结构：CCOC(=O)Nc1nc2ccc(OC)cc2nc1OC
HCID69244324

ethyl N-(3,6-dimethoxyquinoxalin-2-yl)carbamate

C13H15N3O4

PRODUCTS

生成物

1
结构：COc1ccc2nc(NC(=O)N3CCN(c4ccc([N+](=O)[O-])cc4)CC3)c(OC)nc2c1
HCID69244454

未命名化合物

收率 94%

PROCEDURE

实验过程

Ethyl N-(3,6-dimethoxyquinoxalin-2-yl)carbamate and 1-(4-nitrophenyl)piperazine were reacted by the same way with the example 148 to obtain the titled compound (yield, 94%). 1H NMR (300 MHz, CDCl3): δ 3.57-3.65 (m, 8H), 3.90 (s, 3H), 4.01 (s, 3H), 7.06 (d, J=9.4 Hz, 2H), 7.18-7.22 (m, 2H), 7.69 (d, J=8.6 Hz, 2H), 8.09 (d, J=9.4 Hz, 2H), 9.20 (s, 1H).