Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Phenyl isocyanate | HCID 7672 | — |
| Reactant | Methyl 6-aminonicotinate | HCID 737487 | — |
| Product | HCID 57917619 | HCID 57917619 | 104% |
Reaction Steps
To a solution of methyl 6-aminonicotinate (500 mg, 3.29 mmol) in N,N-diemthylformamide (5 mL) was added phenyl isocyanate (358 μL, 3.29 mmol). The mixture was heated to 100° C. for 2 hours and was then concentrated under vacuum to give the title compound (928 mg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US08314091B2 |
|---|
| Source dataset | uspto-grants-2012_11 |
|---|
| ORD ID | ord-94ad57d707064f3e8c411c87b033b174 |
|---|
| Source note | uspto-grants-2012_11 |
|---|
