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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1878551Generated: November 4, 2026

Trifluoroacetic acid → HCID 70999635, compound

https://huagongshe.com/reaction/1878551

Reaction equation

Participants

RoleNameHCIDCharge
ReactantTrifluoroacetic acidHCID 6422—
Reactant3-CarboxybenzaldehydeHCID 12077—
ReactantHCID 70867226HCID 70867226—
SolventEthanolHCID 702—
ProductHCID 70999635HCID 7099963584%

Reaction Steps

There was dissolved, in ethanol (2 mL), trifluoroacetic acid salt of (7-morpholin-4-yl-2-phenyl-pyrazolo[1,5-a]pyrimidin-5-yl)-hydrazine (20.3 mg, 0.0377 mM), then 3-carboxy-benzaldehyde (5.7 mg, 0.038 mM) was added to the solution and the mixture was stirred at room temperature for one hour. This reaction liquid was filtered and the resulting solid was washed with methanol to thus give the title compound (14.0 mg, yield: 84%).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08314098B2
Source datasetuspto-grants-2012_11
ORD IDord-bc2d531147bf4d809e7cd534fd838239
Source noteuspto-grants-2012_11