HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Acid → HCID 70999603, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Acid | HCID 176 | — |
| Reactant | 2-Methyl-7-benzofurancarboxaldehyde | HCID 13201899 | — |
| Reactant | HCID 70867226 | HCID 70867226 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 70999603 | HCID 70999603 | 78% |
Reaction Steps
To a solution of 7-morpholin-4-yl-2-phenyl-pyrazolo[1,5-a]pyrimidin-5-yl-hydrazine (25 mg, 0.081 mM) in absolute ethanol (2.0 mL), there were added 2-methyl-7-formyl-benzofuran (19 mg, 0.12 mM) and acetic acid (2.0 μL) and the mixture was stirred at room temperature for 3 hours. The precipitated solid was recovered through filtration and washed with ethanol to thus give the title compound (28 mg, yield: 78%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08314098B2 |
| Source dataset | uspto-grants-2012_11 |
| ORD ID | ord-e1144ab26cd544adaa9b32b55ed6756b |
| Source note | uspto-grants-2012_11 |