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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1878563Generated: October 31, 2026

Acetic Acid → HCID 70999603, compound

https://huagongshe.com/reaction/1878563

Reaction equation

Participants

RoleNameHCIDCharge
ReactantAcetic AcidHCID 176—
Reactant2-Methyl-7-benzofurancarboxaldehydeHCID 13201899—
ReactantHCID 70867226HCID 70867226—
SolventEthanolHCID 702—
ProductHCID 70999603HCID 7099960378%

Reaction Steps

To a solution of 7-morpholin-4-yl-2-phenyl-pyrazolo[1,5-a]pyrimidin-5-yl-hydrazine (25 mg, 0.081 mM) in absolute ethanol (2.0 mL), there were added 2-methyl-7-formyl-benzofuran (19 mg, 0.12 mM) and acetic acid (2.0 μL) and the mixture was stirred at room temperature for 3 hours. The precipitated solid was recovered through filtration and washed with ethanol to thus give the title compound (28 mg, yield: 78%).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08314098B2
Source datasetuspto-grants-2012_11
ORD IDord-e1144ab26cd544adaa9b32b55ed6756b
Source noteuspto-grants-2012_11