HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 70867226, compound → HCID 70999531, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 70867226 | HCID 70867226 | — |
| Reactant | HCID 86659724 | HCID 86659724 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 70999531 | HCID 70999531 | 85.1% |
Reaction Steps
There was dissolved, in ethanol (2 mL), (7-morpholin-4-yl-2-phenyl-pyrazolo-[1,5-a]pyrimidin-5-yl)-hydrazine (15.1 mg, 0.0487 mM) and then 2-methoxy-benzo-thiazole-4-carbaldehyde (10.4 mg, 0.054 mM) was added to the solution and the mixture was stirred at room temperature for one hour. This reaction liquid was filtered and then the resulting solid was washed with diethyl ether to thus give the title compound (20.1 mg, yield: 85%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08314098B2 |
| Source dataset | uspto-grants-2012_11 |
| ORD ID | ord-df873cf7cab2492d9e4c597c26ac7d5f |
| Source note | uspto-grants-2012_11 |