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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1878569Generated: November 3, 2026

Acetic Acid → HCID 77967083, compound

https://huagongshe.com/reaction/1878569

Reaction equation

Participants

RoleNameHCIDCharge
ReactantAcetic AcidHCID 176—
Reactant3-MethylbenzaldehydeHCID 12105—
ReactantHCID 70999609HCID 70999609—
SolventEthanolHCID 702—
ProductHCID 77967083HCID 7796708385%

Reaction Steps

There was dissolved, in ethanol (2 mL), (2-methyl-7-morpholin-4-yl-pyrazolo-[1,5-a]pyrimidin-5-yl)-hydrazine (24.7 mg, 0.0995 mM), then acetic acid (5.0 μL, 0.087 mM) and 3-methyl-benzaldehyde (12.9 μL, 0.109 mM) were added to the solution and the resulting mixture was stirred at room temperature for 2 hours. This reaction liquid was filtered and the resulting solid was washed with methanol to thus give the title compound (29.6 mg, yield: 85%).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08314098B2
Source datasetuspto-grants-2012_11
ORD IDord-f28679cb7aff4fabb4cbf72ecfa1778e
Source noteuspto-grants-2012_11