HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Acid → HCID 77967083, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Acid | HCID 176 | — |
| Reactant | 3-Methylbenzaldehyde | HCID 12105 | — |
| Reactant | HCID 70999609 | HCID 70999609 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 77967083 | HCID 77967083 | 85% |
Reaction Steps
There was dissolved, in ethanol (2 mL), (2-methyl-7-morpholin-4-yl-pyrazolo-[1,5-a]pyrimidin-5-yl)-hydrazine (24.7 mg, 0.0995 mM), then acetic acid (5.0 μL, 0.087 mM) and 3-methyl-benzaldehyde (12.9 μL, 0.109 mM) were added to the solution and the resulting mixture was stirred at room temperature for 2 hours. This reaction liquid was filtered and the resulting solid was washed with methanol to thus give the title compound (29.6 mg, yield: 85%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08314098B2 |
| Source dataset | uspto-grants-2012_11 |
| ORD ID | ord-f28679cb7aff4fabb4cbf72ecfa1778e |
| Source note | uspto-grants-2012_11 |