HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-acetylbenzaldehyde → HCID 70999655, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-acetylbenzaldehyde | HCID 643436 | — |
| Reactant | HCID 70867116 | HCID 70867116 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 70999655 | HCID 70999655 | 77.4% |
Reaction Steps
There was dissolved, in ethanol (2 mL), (7-morpholin-4-yl-2-pyridin-4-yl-pyrazolo[1,5-a]pyrimidin-5-yl)-hydrazine (30.6 mg, 0.0983 mM), then 3-acetyl-benzaldehyde (14.6 mg, 0.0983 mM) was added to the solution and the mixture was stirred at room temperature overnight. The reaction liquid was filtered and then the resulting solid was washed with diethyl ether to thus give the title compound (33.6 mg, yield: 77%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08314098B2 |
| Source dataset | uspto-grants-2012_11 |
| ORD ID | ord-dfb777223e874aff920bdea5ebf58b86 |
| Source note | uspto-grants-2012_11 |