HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-(Prop-1-en-2-yl)benzaldehyde → HCID 86659734, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-(Prop-1-en-2-yl)benzaldehyde | HCID 19744841 | — |
| Reactant | HCID 70867116 | HCID 70867116 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 86659734 | HCID 86659734 | 62% |
Reaction Steps
There was dissolved, in ethanol (2 mL), (7-morpholin-4-yl-2-pyridin-4-yl-pyrazolo[1,5-a]pyrimidin-5-yl)-hydrazine (30.4 mg, 0.0976 mM), then 3-isopropenyl-benzaldehyde (14.3 mg, 0.0976 mM) was added to the solution and the mixture was stirred at room temperature overnight. The reaction liquid was filtered and then the resulting solid was washed with diethyl ether to thus give the title compound (26.6 mg, yield: 62%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08314098B2 |
| Source dataset | uspto-grants-2012_11 |
| ORD ID | ord-97f3f827e1224f379efb69dce181795c |
| Source note | uspto-grants-2012_11 |