Ammonia → HCID 86761682, compound

Participants

Reaction Steps

Prepared from the product of Example 114A (44.4 mg, 0.080 mmol) according to Method J: 1H NMR (300 MHz, methanol-D4) δ ppm 1.93-1.97 (m, 2H), 2.21 (br s, 1H), 2.36-2.41 (m, 2H), 2.57 (br s, 2H), 3.58 (br s, 2H), 3.66-3.75 (m, 4H), 5.45 (t, J=3.2 Hz, 1H), 7.12 (d, J=9.1 Hz, 1H), 8.13 (dd, J=8.6, 2.5 Hz, 1H), 8.25 (s, 2H), 8.47 (d, J=1.7 Hz, 1H). MS (DCI/NH3) m/z=297 (M+H)+. Anal. Calcd. for C17H20N4O.2 HCl.1.15H2O: C, 52.11; H, 6.30; N, 14.30. Found: C, 52.14; H, 6.33; N, 14.24.

Provenance & Evidence