HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → HCID 11494407, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 2-Bromoethyl methyl ether | HCID 80972 | — |
| Reactant | 4-{2-Fluoro-3-[(trifluoromethyl)sulfonyl]phenyl}piperidine | HCID 57448051 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 11494407 | HCID 11494407 | — |
Reaction Steps
Preparation according to Example 1: 4-{2-fluoro-3-[(trifluoromethyl)sulfonyl]phenyl}-piperidine (0.01 g), acetonitrile (2 ml), potassium carbonate (0.01 g) and 1-bromo-2-methoxyethane (0.01 g). MS m/z (rel. intensity, 70 eV) 369 (M+, 1), 325 (15), 324 (bp), 191 (37), 133 (14).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08314126B2 |
| Source dataset | uspto-grants-2012_11 |
| ORD ID | ord-f214d25567ea4f819eee15af3d7c7e5a |
| Source note | uspto-grants-2012_11 |