HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 67532501, compound → HCID 67533000, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 67532501 | HCID 67532501 | — |
| Solvent | Hydrochloric Acid | HCID 313 | — |
| Product | HCID 67533000 | HCID 67533000 | — |
Reaction Steps
Preparation according to preparation 2: 4-[3-fluoro-2-(trifluoromethyl)phenyl]-1-propylpiperidin-4-ol (2.98 g, 9.8 mmol), hydrochloric acid (40 ml, cone). Yield: 2.37 g. MS m/z (rel. intensity, 70 eV) 305 (M+, 7), 277 (14), 276 (bp), 258 (57), 163 (7).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08314126B2 |
| Source dataset | uspto-grants-2012_11 |
| ORD ID | ord-41ad04da4235449eb8a42833aa4b5bfe |
| Source note | uspto-grants-2012_11 |