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HRID1879029

反应详情

EQUATION

反应方程式

HRID 1879029 的结构方程式

REACTANTS

反应物

2
结构：Cl
HCID313

Hydrochloric Acid

ClH

结构：COC(=O)N1CC=C(c2cccc(S(C)(=O)=O)c2F)CC1
HCID67533257

未命名化合物

PRODUCTS

生成物

1
结构：COC(=O)N1CCC(c2cccc(S(C)(=O)=O)c2F)CC1
HCID67532655

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：[Pd]
催化剂HCID23938

Palladium

Pd

PROCEDURE

实验过程

Preparation according to preparation 18: Methyl 4-[2-fluoro-3-(methylsulfonyl)-phenyl]-3,6-dihydropyridine-1(2H)-carboxylate (1.45 g, 4.6 mmol), palladium on carbon (0.2 g) and hydrochloric acid (0.5 ml, cone). Yield: 0.76 g. MS m/z (relative intensity, 70 eV) 315 (M+, 41), 256 (bp), 236 (54), 141 (43) 114 (50).

WORKUP

后处理

  1. customPreparation
  2. customaccording to preparation 18