HuagongsheHuagongshe Chemistry Print Report · For research reference only
Iodoethane → HCID 67533539, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Iodoethane | HCID 6340 | — |
| Reactant | Sodium borohydride | HCID 4311764 | — |
| Reactant | Benzenesulfonamide, 2-fluoro-N,N-dimethyl-3-(4-pyridinyl)- | HCID 57448067 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 67533539 | HCID 67533539 | — |
Reaction Steps
Preparation according to preparation 6: 2-fluoro-N,N-dimethyl-3-pyridin-4-ylbenzene sulfonamide (0.59 g, 2.11 mmol), 1-iodoethane (3 ml), ethanol (40 ml), sodium borohydride (0.4 g, 10.5 mmol). Yield: 0.27 g. MS m/z (rel. intensity, 70 eV) 312 (M+, bp), 311 (33), 297 (93), 146 (36), 110 (32).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08314126B2 |
| Source dataset | uspto-grants-2012_11 |
| ORD ID | ord-9d0f0032567e478faf13f7c040b58464 |
| Source note | uspto-grants-2012_11 |