HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 57448070, compound → 4-{2-Fluoro-3-[(trifluoromethyl)sulfonyl]phenyl}piperidine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 57448070 | HCID 57448070 | — |
| Catalyst | Platinum oxide (PtO) | HCID 82844 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | 4-{2-Fluoro-3-[(trifluoromethyl)sulfonyl]phenyl}piperidine | HCID 57448051 | — |
Reaction Steps
Preparation according to preparation 9: 4-{2-fluoro-3-[(trifluoromethyl)sulfonyl]phenyl}-pyridine (0.16 g, 0.53 mmol), methanol (10 ml), platinum oxide (0.02 g). Yield: 0.11 g. MS m/z (relative intensity, 70 eV) 311 (M+, 2), 291 (47), 164 (92), 130 (62) 69 (bp).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08314126B2 |
| Source dataset | uspto-grants-2012_11 |
| ORD ID | ord-f6cdfbfdf1ec45fbb65cc0864d64d440 |
| Source note | uspto-grants-2012_11 |