1,3-diethoxyacetone → HCID 86635757, compound

HRID 1879781Notes

Reaction equation

[CH2:1]([O:3][CH2:4][C:5](=O)[CH2:6][O:7][CH2:8][CH3:9])[CH3:2].Cl.[NH2:12][OH:13]>>[CH2:1]([O:3][CH2:4][C:5](=[N:12][OH:13])[CH2:6][O:7][CH2:8][CH3:9])[CH3:2]

Participants

Reactant 2

HCID 2273461,3-diethoxyacetone

HCID 443297Hydroxyamine hydrochloride

Product 1

HCID 86635757HCID 86635757, compound

Procedure

1,3-Diethoxy-propan-2-one oxime was prepared from 1,3-diethoxy-propan-2-one and hydroxylamine hydrochloride using conditions of General Method 1. 1H NMR (400 MHz, DMSO-d6) δ 11.06 (1H, s), 4.18 (2H, s), 3.96 (2H, s), 3.41 (4H, quin, 7.0 Hz), 1.10 (6H, q, 7.1 Hz).

Sources & evidence

ORD record: ord-bbd95fc7965e41d59a37d551a248901b
Source dataset: uspto-grants-2012_11
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US08318705B2

Reaction notes

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