HuagongsheHuagongshe Chemistry Print Report · For research reference only
Cyclohexanone Oxime → Diethyl 1-nitrosocyclohexyl phosphate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Cyclohexanone Oxime | HCID 7517 | — |
| Reactant | Diethyl phosphoric acid | HCID 5166299 | — |
| Reactant | HCID 178418268 | HCID 178418268 | — |
| Product | Diethyl 1-nitrosocyclohexyl phosphate | HCID 44479143 | — |
Reaction Steps
Diethyl 1-nitrosocyclohexyl phosphate was prepared from cyclohexanone oxime, lead tetraacetate and diethyl phosphate using conditions of General Method 3. 1H NMR (400 MHz, benzene-d6) δ 3.90-4.15 (3H, m), 1.24-1.78 (10H, m), 0.88-1.10 (7H, m)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08318705B2 |
| Source dataset | uspto-grants-2012_11 |
| ORD ID | ord-0aee14d156aa43c79268ad6a701855e2 |
| Source note | uspto-grants-2012_11 |