Back
HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1879944Generated: November 2, 2026

HCID 58147973, compound → HCID 136184191, compound

https://huagongshe.com/reaction/1879944

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 58147973HCID 58147973—
SolventTrifluoroacetic acidHCID 6422—
ProductHCID 136184191HCID 13618419193%

Reaction Steps

A solution of 3-Benzyloxy-2-[5-(3-chloro-4-fluoro-benzyl)-thiazol-2-yl]-9-(3-methyl-2-oxo-imidazolidin-1-yl)-7-morpholin-4-yl-pyrido[1,2-a]pyrimidin-4-one (50 mg, 0.076 mmol) in trifluoroacetic acid (1 ml) was refluxed for 3 h. Then trifluoroacetic acid was removed under reduced pressure and MeOH (3 ml) was added. The resulting precipitate was collected by filtration and washed with MeOH to give title compound (40 mg, 93%).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08318732B2
Source datasetuspto-grants-2012_11
ORD IDord-20158c8a5c504de1b95b153f6785f4a0
Source noteuspto-grants-2012_11