Potassium Carbonate → HCID 69308917, compound

Participants

Reaction Steps

An acetone solution of 3-[4-(trifluoromethoxy)phenyl]-1-naphthol (50 mg, 0.166 mmol), methyl 4-(bromomethyl)benzoate (73 mg, 0.32 mmol) and K2CO3 (44 mg, 0.32 mmol) was heated at reflux until no starting material remained by HPLC analysis. The solution was concentrated and the residue purified by silica gel chromatography using a hexanes/ethyl acetate gradient to give the title compound. LCMS1 4.64 min. (M+H)=453

Provenance & Evidence