HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 67530865, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 57687747 | HCID 57687747 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 67530865 | HCID 67530865 | — |
Reaction Steps
(S)-{5-[(4-cyano-benzenesulfonyl)-isobutyl-amino]-6-hydroxy-hexyl}-carbamic acid tert-butyl ester (5) (1.06 g) was dissolved in 50 mL MeOH. HCl (5-6 N in i-prOH, 30 mL) was added and the mixture was stirred overnight at RT. The mixture was evaporated to dryness and used as such in the next reaction.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08318779B2 |
| Source dataset | uspto-grants-2012_11 |
| ORD ID | ord-3ba22c5e85434291af45aef527c17cf7 |
| Source note | uspto-grants-2012_11 |