HRID1880969

反应详情

EQUATION

反应方程式

HRID 1880969 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

A solution of 3-fluoro-5-methoxy-4-nitrobenzoic acid (obtained above), HOAc (5 mL) and MeOH (5 mL) was hydrogenated using a hydrogen balloon overnight. The solution was then filtered through celite and concentrated to a red solid (590 mg, 66%). [M+H] calc'd for C8H8FNO3, 186; found 186.

WORKUP

后处理

  1. filtrationThe solution was then filtered through celite
  2. concentrationconcentrated to a red solid (590 mg, 66%)