HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 67094292, compound → 2-(4-Chlorophenyl)-5,6-dihydroxy-4-nitro-2,3-dihydro-1H-isoindol-1-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 67094292 | HCID 67094292 | — |
| Catalyst | Hydrochloric Acid | HCID 313 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | 2-(4-Chlorophenyl)-5,6-dihydroxy-4-nitro-2,3-dihydro-1H-isoindol-1-one | HCID 15982840 | — |
Reaction Steps
Acetic acid 2-(4-chloro-phenyl)-6-hydroxy-7-nitro-3-oxo-2,3-dihydro-1H-isoindol-5-yl ester (0.24 g raw material) was refluxed in methanol (15 ml) with three drops of concentrated hydrochloric acid for six hours. The reaction mixture was cooled and filtered.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08318785B2 |
| Source dataset | uspto-grants-2012_11 |
| ORD ID | ord-d0368d073e85492f8add1b71dbe63dea |
| Source note | uspto-grants-2012_11 |