HuagongsheHuagongshe Chemistry Print Report · For research reference only
Nitric Acid → 4-Bromo-5-nitroveratrole
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Nitric Acid | HCID 944 | — |
| Reactant | Water | HCID 962 | — |
| Reactant | Benzene, 4-bromo-1,2-dimethoxy- | HCID 76114 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | 4-Bromo-5-nitroveratrole | HCID 170968 | — |
Reaction Steps
To the solution of 4-bromoveratrole (20 g) in acetic acid (50 ml) was added 2M nitric acid (48 ml). It was stirred at room temperature for 30 min and then the reaction solution was poured into water. The resultant solid was filtered, washed with water and dried in vacuum.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08318785B2 |
| Source dataset | uspto-grants-2012_11 |
| ORD ID | ord-7ce940f75bca425eae04142ef7b2c15b |
| Source note | uspto-grants-2012_11 |