Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | HCID 1268893 | HCID 1268893 | — |
| Solvent | Hydrochloric Acid | HCID 313 | — |
| Product | HCID 86633439 | HCID 86633439 | — |
Reaction Steps
5-[1-(4-Benzyloxy-3-methoxy-phenyl)-meth-(Z)-ylidene]-2-thioxo thiazolidin-4-one (38 g) and 2.5M NaOH were warmed at 80° C. for one hour. Next the solution was cooled to 10° C. and poured slowly into 6M HCl-solution (200 ml). The reaction mixture was stirred at room temperature for one hour. The solid was filtered, washed with water and dried under vacuum.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US08318785B2 |
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| Source dataset | uspto-grants-2012_11 |
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| ORD ID | ord-3559c275e1fb4b54bca77f37c46507ee |
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| Source note | uspto-grants-2012_11 |
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