Nitric Acid → HCID 86633440, compound

Participants

Reaction Steps

5-Ethoxy-4-hydroxy-2-nitro-benzaldehyde (1.6 g) was dissolved in dichloromethane (30 ml) and a solution of nitric acid in dichloromethane (2M, 13 ml) was gradually added at a temperature under 30° C. The solution was stirred at room temperature for 10 min and then it was poured into ice-cold water. The organic phase was washed with water and then it was dried and evaporated.

Provenance & Evidence