HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Acid → HCID 67094460, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Acid | HCID 176 | — |
| Reactant | 1,8-Diazabicyclo(5.4.0)undec-7-ene | HCID 81184 | — |
| Reactant | HCID 86633442 | HCID 86633442 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 67094460 | HCID 67094460 | — |
Reaction Steps
(5-Benzyloxy-2-formyl-4-methoxyphenoxy)acetic acid ethyl ester (1.5 g), 1,8-diazabicyclo[5.4.0]undec-7-ene (0.33 g) and acetic acid (0.026 g) in N,N-dimethylformamide (8 ml) were stirred at 100° C. under nitrogen for 5 hours. After cooling to room temperature the mixture was poured in ice water and the precipitate was filtered.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08318785B2 |
| Source dataset | uspto-grants-2012_11 |
| ORD ID | ord-88dfafeaa38040b99c891fadf717b2a2 |
| Source note | uspto-grants-2012_11 |