Ethyl Acetate → HCID 67094182, compound

Participants

Reaction Steps

2-Chlorosulfenyl-4,5-dimethoxybenzoyl chloride (5.0 g) was dissolved in pyridine (30 ml) and methylamine hydrochloride (6.0 g) was added. The mixture was stirred at room temperature for 2 days. Ethyl acetate was added and the mixture was washed with 1 N HCl and water. Ethyl acetate was dried with Na2SO4 and evaporated to dryness. The crude product was purified by flash chromatography eluting with heptane-ethyl acetate (1:9).

Provenance & Evidence