HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylformamide → HCID 67094264, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylformamide | HCID 6228 | — |
| Reactant | Acetic Anhydride | HCID 7918 | — |
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | HCID 67094302 | HCID 67094302 | — |
| Product | HCID 67094264 | HCID 67094264 | — |
Reaction Steps
5,6-Dihydroxy-2-methylbenzo[d]isothiazol-3-one (0.23 g) was suspended in N,N-dimethylformamide and triethylamine (0.47 g) and acetic acid anhydride (0.24 g) were added at 0° C. After stirring at room temperature for one hour the mixture was poured to ice water and the precipitate was filtered.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08318785B2 |
| Source dataset | uspto-grants-2012_11 |
| ORD ID | ord-ac18e8074af8487c9b249364fe669cdf |
| Source note | uspto-grants-2012_11 |