Water → HCID 67094378, compound

Participants

Reaction Steps

(4-Bromo-5,6-dimethoxy-3-methyl-benzo[b]thiophen-2-yl)-morpholin-4-yl-methanone (0.42 g) from Example 33 and copper(I) cyanide (2.0 g) in N,N-dimethylformamide (8 ml) were irradiated in a microwave oven at 150° C. for 1.5 hours. To the mixture water was added and the product was extracted into ethyl acetate. Ethyl acetate was dried and evaporated to dryness.

Provenance & Evidence