Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | 4-(2,2-dimethylpropyl)-2-[1-fluoro-2-(4-pyridin-2-ylphenyl)ethyl]-N,N-dimethyl-1H-imidazole-1-sulfonamide | HCID 66705427 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 66705654 | HCID 66705654 | — |
Reaction Steps
Hydrogen chloride (4 M in 1,4-dioxane) (1 mL, 4 mmol) was added to a solution of 4-(2,2-dimethylpropyl)-2-[1-fluoro-2-(4-pyridin-2-ylphenyl)ethyl]-N,N-dimethyl-1H-imidazole-1-sulfonamide in methanol (1 mL). After stirring at 70° C. for 1 h, volatiles were removed to afford the title compound. (M+H) found: 338.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US08318767B2 |
|---|
| Source dataset | uspto-grants-2012_11 |
|---|
| ORD ID | ord-935edd52b5ad4a9da03c27969343b10c |
|---|
| Source note | uspto-grants-2012_11 |
|---|
