HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic acid 4-acetyl-2-(3,4-dichlorophenyl)thiophen-3-yl ester → 4-{1-[4-Acetoxy-5-(3,4-dichlorophenyl)thiphen-3-yl]ethylidenehydrazinocarbonyl}-2-nitrobenzoic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic acid 4-acetyl-2-(3,4-dichlorophenyl)thiophen-3-yl ester | HCID 67050150 | — |
| Reactant | 4-Hydrazinocarbonyl-2-nitrobenzoic acid | HCID 67050297 | — |
| Product | 4-{1-[4-Acetoxy-5-(3,4-dichlorophenyl)thiphen-3-yl]ethylidenehydrazinocarbonyl}-2-nitrobenzoic acid | HCID 72359960 | — |
Reaction Steps
The title compound was prepared from acetic acid 4-acetyl-2-(3,4-dichlorophenyl)thiophen-3-yl ester (39.5 mg, 0.12 mmol) and 4-hydrazinocarbonyl-2-nitrobenzoic acid (40.5 mg, 0.18 mmol) following the procedure described in the synthetic example 185.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08318796B2 |
| Source dataset | uspto-grants-2012_11 |
| ORD ID | ord-b25cf7b02bd84e05b3a07667cfef1a7f |
| Source note | uspto-grants-2012_11 |