HuagongsheHuagongshe Chemistry Print Report · For research reference only
Lithium Hydroxide → HCID 57904202, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Lithium Hydroxide | HCID 3939 | — |
| Reactant | HCID 57904271 | HCID 57904271 | — |
| Solvent | Methanol | HCID 887 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 57904202 | HCID 57904202 | — |
Reaction Steps
4-(1-(2-(Trifluoromethyl)phenylsulfonyl)piperidin-2-yl)butanoic acid methyl ester (3.5 g, 8.9 mmol, 1 eq.) was dissolved in water (25 ml) and methanol (35 ml). Lithium hydroxide (1 g, 44.5 mmol, 5 eq.) was added, while stirring. The mixture was stirred at room temperature for 24 h.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08318769B2 |
| Source dataset | uspto-grants-2012_11 |
| ORD ID | ord-99a7261f9de242388becd0442c27055f |
| Source note | uspto-grants-2012_11 |