HuagongsheHuagongshe Chemistry Print Report · For research reference only
Lithium Hydroxide → HCID 57904137, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Lithium Hydroxide | HCID 3939 | — |
| Reactant | HCID 57904254 | HCID 57904254 | — |
| Solvent | Methanol | HCID 887 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 57904137 | HCID 57904137 | — |
Reaction Steps
4-(1-(2-Chloro-6-methylphenylsulfonyl)piperidin-2-yl)butanoic acid methyl ester (2.7 g, 7.3 mmol, 1 eq.) was dissolved in water (20 ml) and methanol (30 ml). Lithium hydroxide (0.87 g, 36.5 mmol, 5 eq.) was added, while stirring. The mixture was stirred at room temperature for 24 h.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08318769B2 |
| Source dataset | uspto-grants-2012_11 |
| ORD ID | ord-8721d5aaf714412ead194404ce2f1cd6 |
| Source note | uspto-grants-2012_11 |