HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylamine → 5-(Dimethylamino)-2-nitrobenzoic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylamine | HCID 674 | — |
| Reactant | 5-Chloro-2-nitrobenzoic acid | HCID 17286 | — |
| Product | 5-(Dimethylamino)-2-nitrobenzoic acid | HCID 12715793 | — |
Reaction Steps
Concretely, 5-chloro-2-nitrobenzoic acid is dissolved in a dimethylamine aqueous solution and heated to produce 5-dimethylamino-2-nitrobenzoic acid. Hydrochloric acid is added to the reaction solution to precipitate out the product as a solid material. The solid material is separated to obtain 5-dimethylamno-2-nitrobenzoic acid almost quantitatively.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08318975B2 |
| Source dataset | uspto-grants-2012_11 |
| ORD ID | ord-d51104c16ad949ca8411ee3dabdfe32d |
| Source note | uspto-grants-2012_11 |