HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl 4-chloro-3,5-dinitrobenzoate → 4-(2-Fluoro-5-methyl-pyridin-3-yl)-3,5-dinitro-benzoic acid methyl ester
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl 4-chloro-3,5-dinitrobenzoate | HCID 96161 | — |
| Reactant | 4-(2-Fluoro-5-methyl-pyridin-3-yl)-3,5-dinitro-benzonitrile | HCID 58880175 | — |
| Product | 4-(2-Fluoro-5-methyl-pyridin-3-yl)-3,5-dinitro-benzoic acid methyl ester | HCID 58880174 | 94% |
Reaction Steps
The title compound was prepared from 4-chloro-3,5-dinitro-benzoic acid methyl ester in 94% yield according to the procedure outline for the preparation of Compound 122. MS (ES) [m+H] calc'd for C14H10FN3O6, 336; found 336.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08318939B2 |
| Source dataset | uspto-grants-2012_11 |
| ORD ID | ord-86c225c99aa14e6fa61db222c7251018 |
| Source note | uspto-grants-2012_11 |