HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-Amino-3-methyl-9H-pyrido[2,3-b]indole-7-carbonitrile → 5-Amino-3-methyl-9H-pyrido[2,3-b]indole-7-carboxylic acid methyl ester
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-Amino-3-methyl-9H-pyrido[2,3-b]indole-7-carbonitrile | HCID 16124311 | — |
| Reactant | 4-(2-Fluoro-5-methyl-pyridin-3-yl)-3,5-dinitro-benzoic acid methyl ester | HCID 58880174 | — |
| Product | 5-Amino-3-methyl-9H-pyrido[2,3-b]indole-7-carboxylic acid methyl ester | HCID 58880122 | 88% |
Reaction Steps
The title compound was prepared in 88% yield from example Compound 128 according to the procedure outlined for the preparation of Compound 124. MS (ES) [m+H] calc'd for C14H13N3O2, 256; found 256.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08318939B2 |
| Source dataset | uspto-grants-2012_11 |
| ORD ID | ord-0ea0c055e4db4ca19e6bb37ea984ed96 |
| Source note | uspto-grants-2012_11 |