HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → HCID 86084132, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | N-bromobutanimide | HCID 67184 | — |
| Reactant | HCID 86084129 | HCID 86084129 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 86084132 | HCID 86084132 | — |
Reaction Steps
5.4 g of 1,6-dinaphthalene-2-yl-3-phenylpyrene was dispersed into 60 ml of DMF, and 1.9 g NBS in DMF solution was dropped therein at room temperature. After 3 days reaction, 150 ml of water was added to it and the deposited crystal was filtrated, followed by water and ethanol washing of the crystal.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08318995B2 |
| Source dataset | uspto-grants-2012_11 |
| ORD ID | ord-98ad62204d5f408e9c67bf99d51f494a |
| Source note | uspto-grants-2012_11 |