Tetrahydrofuran → HCID 178479811, Verbindung

HRID 1883105Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 1883105
[OH:1][C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][N:3]=1.[CH2:8]([N:10](CC)CC)C.[Pt:15]([Cl:19])(Cl)(Cl)[Cl:16].[CH2:20]1[CH2:24][O:23][CH2:22][CH2:21]1>>[N:3]1[CH:4]=[CH:5][CH:6]=[CH:7][C:2]=1[O:1][Pt:15]([Cl:19])([Cl:16])[O:23][C:24]1[CH:20]=[CH:21][CH:22]=[CH:8][N:10]=1

Komponenten

5

Edukt 4

HCID 8028TetrahydrofuranHCID 8471TriethylamineHCID 26031Platinum tetrachlorideHCID 178516071HCID 178516071, Verbindung

Produkt 1

HCID 178479811HCID 178479811, Verbindung

Versuchsvorschrift

To a solution of 0.02 moles of 2-hydroxypyridine and 0.02 moles of triethylamine in 50 mL of THF, a solution of 0.01 moles of platinum tetrachloride is added dropwise at 0° C. The solution is then stirred overnight at room temperature. After filtration, the THF solution is evaporated and the product is extracted from the residue. Polymers may be produced using the catalyst by following the procedure of Example 4.

Aufarbeitung

  1. filtrationAfter filtration
  2. customthe THF solution is evaporated
  3. extractionthe product is extracted from the residue
  4. customPolymers may be produced

Quellen und Nachweise

ORD-Eintrag
ord-836569bce09a4e0993cbedf0b4c03976
Quelldatensatz
uspto-grants-2004_07
Patentnummer
US06759493B1

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