HuagongsheHuagongshe Chemistry Print Report · For research reference only
Iodine → HCID 13487918, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Iodine | HCID 807 | — |
| Reactant | Dimethyl Sulfate | HCID 6497 | — |
| Reactant | Thiophene-3-carboxylic acid | HCID 6918 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | Lithium diisopropylamide | HCID 2724682 | — |
| Product | HCID 13487918 | HCID 13487918 | — |
Reaction Steps
Thiophene-3-caboxylic acid was treated with lithium diisopropylamide and iodine, and the resultant was reacted with (CH3)2SO4 in the presence of K2CO3 to give methyl 4-iodothiophene-3-carboxylate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06759429B2 |
| Source dataset | uspto-grants-2004_07 |
| ORD ID | ord-f954eaa72c4346728572205da18892ea |
| Source note | uspto-grants-2004_07 |