HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Pyrrolidone → HCID 11367213, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Pyrrolidone | HCID 12025 | — |
| Reactant | 2-Bromothiophene | HCID 13851 | — |
| Product | HCID 11367213 | HCID 11367213 | 95% |
Reaction Steps
Using general procedure C, 2-bromothiophene was coupled with 2-pyrrolidinone with the reaction time of 16 h. Chromatography gave 158 mg (95%) of the title compound as a solid. 1H NMR (CDCl3, 300 MHz): δ 6.94−6.86 (m, 2H), 6.53 (br s, 1H), 3.89 (t, 2H, J=7.2 Hz), 2.63 (t, 2H, J=8.1 Hz), 2.24 (p, 2H, J=7.5 Hz).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06759554B2 |
| Source dataset | uspto-grants-2004_07 |
| ORD ID | ord-63a9adb8e40a4e1680a1d0d2bede7cba |
| Source note | uspto-grants-2004_07 |