HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 53784447, compound → HCID 23509923, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 53784447 | HCID 53784447 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 23509923 | HCID 23509923 | 99.2% |
Reaction Steps
3-(4-Nitro-phenyl)-2-(3-trifluoromethyl-phenyl)-acrylic acid (9.9 g, 29 mmol) was hydrogenated in methanol using palladium/charcoal (10%) as the catalyst in 13 hours. The catalyst was filtered off and the filtrate was evaporated to give 8.9 g of the desired product (98% yield). MS m/z: 310.2 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06759420B1 |
| Source dataset | uspto-grants-2004_07 |
| ORD ID | ord-b68d861231ef4cb681afed10b11e25d7 |
| Source note | uspto-grants-2004_07 |