HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Butyn-1-ol → HCID 57159696, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Butyn-1-ol | HCID 12991 | — |
| Reactant | HCID 53962319 | HCID 53962319 | — |
| Product | HCID 57159696 | HCID 57159696 | 98% |
Reaction Steps
According to the procedure of Example 5 242 mg (0.58 mmol) of the product of Example 42 and 0.049 ml (0.65 mmol) of 2-butyn-1-ol provides 0.239 g (98%) of 4-[(4-but-2-ynyloxy-benzenesulfonyl)-methyl-amino]-5-methyl-biphenyl-3-carboxylic acid methyl ester. Electrospray Mass Spec: 464.2 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06762178B2 |
| Source dataset | uspto-grants-2004_07 |
| ORD ID | ord-46454364295d4f4796b2dc36ebcbed83 |
| Source note | uspto-grants-2004_07 |