HCID 23508555, compound → HCID 23508418, compound

Participants

Reaction Steps

The procedure of Preparation Example 2 was repeated, except that 71 mg of 4-cyano-N-(4-methoxybenzyl)-N-methylbenzamide was used in place of 4′-methoxy-2-biphenylacetonitrile, and toluene was used in place of methylene chloride. The resulting crude product was purified by TLC (using a 4:1 mixture of chloroform and acetone as the developing solvent) to obtain 53 mg of 4-cyano-N-(4-hydroxybenzyl)-N-methylbenzamide.

Provenance & Evidence