HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 69859806, compound → HCID 23508311, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 69859806 | HCID 69859806 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 23508311 | HCID 23508311 | 86.8% |
Reaction Steps
A solution of ethyl 3-[7-acetylamino-indan-4-yl]-but-2-enoate (1.9 g, Reference Example 7) in ethanol (200 mL) was hydrogenated over 10% palladium on charcoal for 16 hours. The mixture was filtered through diatomaceous earth and the filtrate was evaporated to give the title compound (1.66 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06762199B2 |
| Source dataset | uspto-grants-2004_07 |
| ORD ID | ord-434ee3510dec4a728e8def25a85bbf26 |
| Source note | uspto-grants-2004_07 |