p-Fluoronitrobenzene → HCID 23507448, compound
Reaction equation
F[C:2]1[CH:7]=[CH:6][C:5]([N+:8]([O-:10])=[O:9])=[CH:4][CH:3]=1.[CH3:11][N:12]([CH3:26])[CH2:13][CH2:14][NH:15][S:16]([CH2:19][C:20]1[CH:25]=[CH:24][CH:23]=[CH:22][CH:21]=1)(=[O:18])=[O:17].[H-].[Na+]>>[CH3:11][N:12]([CH3:26])[CH2:13][CH2:14][N:15]([C:2]1[CH:7]=[CH:6][C:5]([N+:8]([O-:10])=[O:9])=[CH:4][CH:3]=1)[S:16]([CH2:19][C:20]1[CH:25]=[CH:24][CH:23]=[CH:22][CH:21]=1)(=[O:17])=[O:18]Participants
4
Procedure
Prepared from 1-fluoro-4nitro-benzene, N-(2-dimethylamino-ethyl)-C-phenylmethanesulphonamide and sodium hydride as base
Sources & evidence
- ORD record
- ord-c177ff8c605b4b6c9db224b2ab1d341a
- Source dataset
- uspto-grants-2004_07
- Patent number
- US06762180B1
Reaction notes
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