HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethylamine → HCID 4719099, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethylamine | HCID 6341 | — |
| Reactant | 4-Nitrobenzyl bromide | HCID 66011 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 4719099 | HCID 4719099 | — |
Reaction Steps
6.0 g of 4-nitrobenzyl bromide are dissolved in 25 ml of ethanol, combined with 25 ml of 10% ethanolic ethylamine solution and refluxed for 2 hours. Then the solution is concentrated by rotary evaporation, the residue is taken up with methylene chloride and washed with dilute sodium hydroxide solution. Finally the organic phase is evaporated down.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06762180B1 |
| Source dataset | uspto-grants-2004_07 |
| ORD ID | ord-d60d15ae4e304301a742ad5b3111fd2e |
| Source note | uspto-grants-2004_07 |