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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1883770Generated: November 1, 2026

Ethylamine → HCID 4719099, compound

https://huagongshe.com/reaction/1883770

Reaction equation

Participants

RoleNameHCIDCharge
ReactantEthylamineHCID 6341—
Reactant4-Nitrobenzyl bromideHCID 66011—
SolventEthanolHCID 702—
ProductHCID 4719099HCID 4719099—

Reaction Steps

6.0 g of 4-nitrobenzyl bromide are dissolved in 25 ml of ethanol, combined with 25 ml of 10% ethanolic ethylamine solution and refluxed for 2 hours. Then the solution is concentrated by rotary evaporation, the residue is taken up with methylene chloride and washed with dilute sodium hydroxide solution. Finally the organic phase is evaporated down.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06762180B1
Source datasetuspto-grants-2004_07
ORD IDord-d60d15ae4e304301a742ad5b3111fd2e
Source noteuspto-grants-2004_07