HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 86587026, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | Chloromethyl ethyl ether | HCID 18523 | — |
| Reactant | 5-Norbornene-2-carboxylic acid | HCID 78949 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 86587026 | HCID 86587026 | 89% |
Reaction Steps
1 mol of 5-norbornene-2-carboxylic acid was dissolved in 1.5 l of THF, and 1.1 mol of triethylamine and 1.1 mol of chloromethylethylether were added thereto. The reaction was carried out at room temperature for 6 hours. After completion of the reaction, the resultant mixture was distilled under reduced pressure to provide 5-norbornene-2-ethoxymethylcarboxylate (ANCA) in 89% yield.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06762268B2 |
| Source dataset | uspto-grants-2004_07 |
| ORD ID | ord-0aa577e944d746daa449f8efd5df18c6 |
| Source note | uspto-grants-2004_07 |