HuagongsheHuagongshe Chemistry Print Report · For research reference only
p-Fluoronitrobenzene → 1-Nitro-4-{[4-(trifluoromethyl)benzyl]oxy}benzene
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | p-Fluoronitrobenzene | HCID 9590 | — |
| Reactant | 4-(Trifluoromethyl)benzenemethanol | HCID 67684 | — |
| Reactant | 1-(3-Fluorobenzyloxy)-4-nitro-benzene | HCID 22137915 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | 1-Nitro-4-{[4-(trifluoromethyl)benzyl]oxy}benzene | HCID 2743792 | — |
Reaction Steps
Prepared in analogy to 1-(3-fluorobenzyloxy)-4-nitro-benzene, starting from 4-fluoro nitrobenzene and 4-trifluoromethyl benzyl alcohol. Yield after recristallisation from methanol: 82% of a brownish solid. Mp=80.5-81.5° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06762320B2 |
| Source dataset | uspto-grants-2004_07 |
| ORD ID | ord-81efb0f73cfe484fbf072873c52f0f78 |
| Source note | uspto-grants-2004_07 |